The synthesis of lemonile perfume from litsea cubeba oil is newly studied and re-formed.
本文对利用山苍子油中柠檬醛合成柠檬腈香料进行了新探和改进。
Lemonile was manufactured by the dehydration of citral oxime obtained by the reaction of hydroxylamine sulfuride and citral abstracted from litsea cubeba oil.
从山苍子提取出的柠檬醛,与硫酸羟胺反应生成柠朦肟,脱水后可得到柠檬腈。
The catalytic dehydration of lemonile with various alkalis and PTC was studied. The optimal conditions dehydration to lemonile for KOH TBAB catalytic by orthogonal design were determined.